X-ray diffraction of materials under ramp compression on the Thor pulsed-power generator

ORAL

Abstract

Thor is a pulsed-power generator which uses magnetic loading to produce well-controlled ramp compression for high-pressure research of material response and equation-of-state. Thor has recently been configured with a compact x-ray diffraction (XRD) capability to allow investigation of atomic-scale response under dynamic compression, such as crystal lattice compression, onset of plastic flow, strength-strain rate dependence, structural phase transitions, and density of crystal defects such as dislocations. We describe our cost effective, compact x-ray source implementation and present ambient and dynamic data for several materials with solid-solid phase transformations in the 1 to 10 GPa pressure range (e.g. CdS, Zr). We have found the combination of magnetically-driven ramp compression with single, short-pulse XRD diagnostic to be a powerful new capability for the dynamic materials research.

*Sandia National Laboratories is a multimission laboratory managed and operated by National Technology & Engineering Solutions of Sandia, LLC, a wholly owned subsidiary of Honeywell International Inc., for the U.S. Department of Energy's National Nuclear Security Administration under contract DE-NA0003525. This work was supported by the Laboratory Directed Research and Development program at Sandia National Laboratories.

Publication: "A compact x-ray diffraction system for dynamic compression experiments on pulsed-power generators", T. Ao, D.V. Morgan, B.S. Stoltzfus, K.N. Austin, J. Usher, E. Breden, L.M. Pacheco, S. Dean, J.L. Brown, S. Duwal, H. Fan, P. Kalita, M.D. Knudson, M. A. Rodriguez, and J.M.D. Lane, Rev. Sci. Instrum. (submitted).

Presenters

  • Tommy Ao

    • Sandia National Laboratories

Authors

  • Tommy Ao

    • Sandia National Laboratories
  • Dane V Morgan

    • MSTS, Albuquerque NM USA
    • DOE
    • Mission Support and Technical Services, LLC
  • J Matthew D Lane

    • Sandia National Laboratories
  • Kevin N Austin

    • Sandia National Laboratories
  • Eric W Breden

    • Sandia National Laboratories
  • Justin L Brown

    • Sandia National Laboratories
  • Sakun Duwal

    • Sandia National Laboratories
  • Hongyou Fan

    • Sandia National Laboratories
  • Patricia Kalita

    • Sandia National Laboratory
    • Sandia National Laboratories
  • Marcus Knudson

    • Sandia National Laboratories
    • Sandia National Laboratories, Albuquerque NM 87185, USA
  • Lena M Pacheco

    • Sandia National Laboratories
  • Mark A Rodriguez

    • Sandia National Laboratories
  • Brian S Stoltzfus

    • Sandia National Laboratories
  • Joshua M Usher

    • Sandia National Laboratories