High-Speed Rotational Diamond Anvil Cell (HS-RDAC) for Shear Deformation Study

ORAL

Abstract

A first of its kind high-speed rotational diamond anvil cell (HS-RDAC) has been tested at HPCAT beamlines. The device basically consists of a support diamond anvil and an opposing high-speed rotating diamond anvil, of which the rotation speed can be adjusted up to kilo-rpm level. The development is aimed at enabling a new platform to emulate deformation-based solid-state processing under moderate uniaxial compression condition and provide an experimental approach for predictive understanding of the fundamental atomic scale mechanism of mass and energy transfer under shear deformation conditions. As a pilot test, solid-state mixing of Cu-Ni binary powders has been tried, and the time-dependent lattice strain evolution and spatial variation of defect density across the sample dimension have been investigated. The study provides new insights into how interface mass transfer could be accelerated under shear deformation.

*HPCAT operations are supported by DOE-NNSA's Office of Experimental Sciences. The Advanced Photon Source is a U.S. Department of Energy (DOE) Office of Science User Facility operated for the DOE Office of Science by Argonne National Laboratory under Contract No. DE-AC02-06CH11357. This research is supported by the Solid Phase Process Science Initiative (SPPSi), under the Laboratory Directed Research and Development (LDRD) Program at Pacific Northwest National Laboratory (PNNL). PNNL is a multi-program national laboratory operated for the U.S. Department of Energy (DOE) by Battelle Memorial Institute under Contract No. DE-AC05-76RL01830.

Presenters

  • Changyong Park

    • HPCAT, X-ray Science Division, Argonne National Laboratory
    • Argonne National Laboratory

Authors

  • Changyong Park

    • HPCAT, X-ray Science Division, Argonne National Laboratory
    • Argonne National Laboratory
  • Arun Devaraj

    • Pacific Northwest National Laboratory
  • Tingkun Liu

    • Pacific Northwest National Laboratory
  • Stanislav Sinogeikin

    • DAC Tools LLC