Two-Dimensional Transition Metal Dichalcogenides: Controlled Synthesis and Optical Characterization

ORAL

Abstract

Chemical vapor deposition (CVD) is a bottom-up approach suitable for the synthesis of MoS$_{2}$ and WS$_{2}$ monolayers. In order to extend the application of CVD, we modified the precursors used during the deposition. We show that by using mixed transition metal precursors of MoS$_{2}$/WO$_{3}$ powders, alloyed monolayers of Mo$_{x}$W$_{1-x}$S$_{2}$ islands can be synthesized exhibiting a compositional gradient and a tunable optical band gap, as confirmed by Raman and photoluminescence measurements. We further show that adding tellurium powders into the transition metal precursors can lead to a 200 $^{o}$C reduction in the synthesis temperature for MoS$_{2}$ and WS$_{2}$ monolayers. The materials synthesized at a reduced temperature maintain a high degree of crystallinity and optical properties.

Authors

  • Zhong Lin

    • The Pennsylvania State University
  • Yongji Gong

    • Rice University
  • Gonglan Ye

    • Rice University
  • Gang Shi

    • Rice University
  • Michael Thee

    • The Pennsylvania State University
  • Ana Laura Elias

    • The Pennsylvania State University
    • Department of Physics and Materials Science and Engineering, Penn-State University
  • Nestor Perea-Lopez

    • The Pennsylvania State University
  • Simin Feng

    • Penn State University
    • The Pennsylvania State University
  • Yu Lei

    • The Pennsylvania State University
  • Chanjing Zhou

    • The Pennsylvania State University
  • Kazunori Fujisawa

    • The Pennsylvania State University
  • Victor Carozo

    • The Pennsylvania State University
  • Robert Vajtai

    • Rice University
  • Humberto Terrones

    • Rensselaer Polytechnic Institute
  • Zheng Liu

    • Nanyang Technological University
  • Pulickel M. Ajayan

    • Rice University
  • Mauricio Terrones

    • The Pennsylvania State University