High pressure synthesis of single crystalline MgB$_{2}$

ORAL

Abstract

We report the results of single crystal growth of MgB$_{2}$.~ A high pressure furnace, using a 19 mm truncation edge length, cubic anvil capable of reaching 3.3 GPa and 2000 C was used to grow crystals of MgB$_{2}$ out of the Mg-B-N ternary.~ Design, setup, and calibration will be discussed as well as correlations between pressure and temperature profiles and crystal size.~ Results of measurements of penetration depth and H$_{c2}$(T) on single crystals will be shown as well as the results of initial doping studies.

*Work at the Ames Laboratory was supported by the Department of Energy, Basic Energy Sciences under Contract No. DE-AC02-07CH11358.

Authors

  • M. Tillman

    • Ames Lab / Iowa State University
  • G. Lapertot

    • CEA-Grenoble, DRFMC/SPSMS/IMAPEC
  • R. Prozorov

    • Ames Lab / Iowa State University
  • C. Martin

    • Ames Lab / Iowa State University
  • S.L. Bud'ko

    • Ames Lab / Iowa State University
  • P.C. Canfield

    • Ames Lab / Iowa State University