Microwave plasma produced carbon nanostructures

POSTER

Abstract

A microwave, atmospheric argon plasma driven by surface waves has been used for synthesizing carbon nanostructures by passing vaporized ethanol through the plasma. The method is based on sending vaporized ethanol molecules through a microwave argon plasma environment, where decomposition of ethanol molecules takes place and carbon atoms are created. These carbon atoms agglomerate subsequently in the outlet gas stream to form nanostructures that are collected by nylon membrane filters. External, forced cooling/heating has been applied using a cryostatic system to fix the temperature in the nucleation zone of the plasma reactor. The synthesized carbon nanostructures were analyzed by high-resolution transmission electron microscopy (HRTEM), X-ray photoelectron spectroscopy (XPS), and micro-Raman spectroscopy. Graphene sheets and carbon nanoparticles have been selectively synthesized through the control of the outlet plasma stream temperature.

Authors

  • Julio Henriques

    • Institute of Plasmas and Nuclear Fusion, Instituto Superior Tecnico, Technical University of Lisbon, Portugal
  • Elena Tatarova

    • Institute of Plasmas and Nuclear Fusion, Instituto Superior Tecnico, Technical University of Lisbon, Portugal
  • Claudia Luhrs

    • Department of Mechanical and Aerospace Engineering, Naval Postgraduate School,Monterey, CA 93943, USA
  • Jonathan Phillips

    • Department of Mechanical and Aerospace Engineering, Naval Postgraduate School,Monterey, CA 93943, USA
  • Ana Rego

    • Centro de Quimica-Fisica Molecular and IN, Instituto Superior Tecnico, Technical University of Lisbon, Portugal
  • Ana Ferraria

    • Centro de Quimica-Fisica Molecular and IN, Instituto Superior Tecnico, Technical University of Lisbon, Portugal
  • Miroslav Abrashev

    • Faculty of Physics, Sofia University, Sofia, Bulgaria
  • Ana Dias

    • Institute of Plasmas and Nuclear Fusion, Instituto Superior Tecnico, Technical University of Lisbon, Portugal
  • Carlos Ferreira

    • Institute of Plasmas and Nuclear Fusion, Instituto Superior Tecnico, Technical University of Lisbon, Portugal